1: 5-hydroxypentyne With n-butyllithium in tetrahydrofuran; toluene T=-68°C; 1 h; 2: triethylsilyl chloride in tetrahydrofuran; toluene T=-68 - 20°C; 20 h; 3: With hydrogenchloride in tetrahydrofuran; toluene T=20°C; 48 h;
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