反应条件
1: 1.) LiNH2 / 1.) ammonia, 2.) THF
2: 70 percent / PCC / CH2Cl2
3: 1.) NaH / 1.) THF, RT, 1 h, 2a.) 0 deg C, 1 h, 2b.) RT, 4 h
4: K, naphthalene, hexamethyldisilazane / tetrahydrofuran / 4 h / -78 °C
5: LiAlH4 / diethyl ether
6: 81 percent / PPh3Br2, pyridine / CH2Cl2 / 4 h
View Scheme
参考文献
Chattopadhyay, A.; Mamdapur, B.
Synthetic Communications, 1990 , vol. 20, # 15 p. 2225 - 2234
