反应条件
1: triethylamine / dichloromethane / 24 h / 0 - 20 °C / |Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); isopropylamine; copper(l) iodide / ethylene glycol dimethyl ether / 3.5 h / 70 °C / |Inert atmosphere
3: hydrogen; palladium 10 on activated carbon / ethyl acetate / 0.75 h / |Inert atmosphere
4: diisobutylaluminium hydride / tetrahydrofuran / 0.25 h / 0 °C
5: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 2 h / 0 °C
6: sodium acetate; hydroxylamine hydrochloride / isopropyl alcohol / 1.5 h / 20 °C
7: Acid orange 52; sodium cyanoborohydride; hydrogenchloride / methanol / 1 h / 20 °C
8: sodium cyanoborohydride / tert-butyl alcohol / 16 h / |Inert atmosphere; |Sealed tube; |Microwave irradiation
9: zinc; trifluoroacetic acid; water / dichloromethane / 20 °C
View Scheme
参考文献
Dion, Isabelle; Vincent-Rocan, Jean-Francois; Zhang, Lei; Cebrowski, Pamela H.; Lebrun, Marie-Eve; Pfeiffer, Jennifer Y.; Bedard, Anne-Catherine; Beauchemin, Andre M.
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12735 - 12749
