反应条件
1: 1) LiNH2 / 1) NH3(l), 3 h; 2) abs THF, 20-25 deg C, 13 h.
2: 85 percent / LiAlH4, / bis-(2-methoxy-ethyl) ether / 11.5 h / Heating
3: 90 percent / pyridinium chlorochromate / CH2Cl2
4: 1) sodium bis(trimethylsilyl)amide / 1) abs. THF; 2) abs. THF
5: 70 percent / glacial acetic acid / Heating
View Scheme
参考文献
Kovalev, B. G.; Avdeeva, L. A.; Sorochinskaya, A. M.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 4 p. 641 - 646
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 4 p. 713 - 718
