1-(4-溴苯基)-1-乙醇合成路线 (共 105 条)
反应条件
zirconium(IV) hydrous oxide hydroxide; isopropyl alcohol T=130°C; Meerwein-Ponndorf-Verley Reduction; 0.366667 h;
参考文献
Battilocchio, Claudio; Hawkins, Joel M.; Ley, Steven V.
Organic Letters, 2013 , vol. 15, # 9 p. 2278 - 2281
反应条件
[RuCl2(triphenylphosphine)((6-((3,5-dimethyl-pyrazol-1-yl)pyridin-2-yl)methylene)-p-tolyl-amine)]*0.5Et2O; potassium isopropoxide T=82°C; P=750.075 Torr; 1.16667 h; Inert atmosphere;
参考文献
Ye, Wenjing; Zhao, Miao; Du, Wangming; Jiang, Quanbin; Wu, Kaikai; Wu, Ping; Yu, Zhengkun
Chemistry - A European Journal, 2011 , vol. 17, # 17 p. 4737 - 4741
反应条件
diphosphorous tetraiodide; tetraethylammonium bromide; water in dichloromethane T=20°C; 6 h; regioselective reaction;
参考文献
Telvekar, Vikas N.; Rane, Rajesh A.
Synthetic Communications, 2010 , vol. 40, # 14 p. 2108 - 2112
反应条件
bis(acetylacetonate)nickel(II); triphenylphosphine in tetrahydrofuran; hexane T=0°C; 21 h;
参考文献
Ichiyanagi, Tsuyoshi; Kuniyama, Satoru; Shimizu, Makoto; Fujisawa, Tamotsu
Chemistry Letters, 1998 , # 10 p. 1033 - 1034
反应条件
tert.-butylhydroperoxide; WO3 in water T=80°C; 12 h;
参考文献
Shaikh, Tanveer Mahammad Ali; Sudalai, Arumugam
European Journal of Organic Chemistry, 2008 , # 29 p. 4877 - 4880
反应条件
1: With formic acid; toluene-4-sulfonic acid in water T=100°C; 5 h; Inert atmosphereSealed tube; 2: With chloro-(pentamethylcyclopentadienyl)-{5-methoxy-2-{1-[(4-methoxyphenyl)imino-N]ethyl}phenyl-C}-iridium(lll); water; sodium formate T=20 - 80°C; pH=3.5; 6 h;
参考文献
Li, Jia; Wang, Chao; Xue, Dong; Wei, Yawen; Xiao, Jianliang
Green Chemistry, 2013 , vol. 15, # 10 p. 2685 - 2689
反应条件
1: With 1-bromo-butane; sodium tetrahydroborate; Aliquatreg; 336 T=20°C; Addition; Hydroboration; 16 h; 2: With sodium hydroxide; dihydrogen peroxide T=40°C; Oxidation; 1 h;
参考文献
Synlett, , # 7 p. 997 - 998
反应条件
(tetrakis(N-methyl-4-pyridinium)porphyrinato)-manganese(III) phosphotungstate; PhIO T=30°C; 1 h; Ionic liquid;
参考文献
Monatshefte fur Chemie, , vol. 141, # 8 p. 859 - 865
反应条件
1: With 1,10-phenanthroline; oxygen; copper diacetate; triethylamine in toluene; acetonitrile T=20°C; 2: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 1 h;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
反应条件
Oxonereg;; potassium bromide in nitromethane T=50°C; 3 h;
参考文献
Organic Letters, , vol. 14, # 9 p. 2414 - 2417