1-(4-溴苯基)-1-乙醇合成路线 (共 105 条)
反应条件
n-butyllithium; diethyl ether
anschliessend Behandeln mit festem Kohlendioxid;
参考文献
Gilman; Melstrom
Journal of the American Chemical Society, 1948 , vol. 70, p. 4177
反应条件
0.0666667 h; microwave irradiation;
参考文献
Lee, Jong Chan; Lee, Ji Young; Lee, Seung Jun
Tetrahedron Letters, 2004 , vol. 45, # 25 p. 4939 - 4941
反应条件
sodium hydride in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Bakke, Jan M.; Froehaug, Astrid E.
Acta Chemica Scandinavica, 1995 , vol. 49, # 8 p. 615 - 622
反应条件
(SIPr)Pd(Py)Cl2; potassium tert-butylate in toluene
T=100°C; 12 h; Inert atmosphere;
参考文献
Shi, Yanhui; Cai, Zhengyuan; Guan, Pei; Pang, Guangsheng
Synlett, 2011 , # 14 art. no. W09311ST, p. 2090 - 2096
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C
2: iodine / neat (no solvent) / 2 h / 85 °C
View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999