BETA-(4-CHLOROPHENYL)GLUTARIC ANHYDRIDE合成路线 （共 6 条）
反应条件
acetyl chloride 1 h; Reflux;
参考文献
Froehner, Wolfgang; Lopez-Garcia, Laura A.; Neimanis, Sonja; Weber, Nadja; Navratil, Jeanette; Maurer, Frauke; Stroba, Adriana; Zhang, Hua; Biondi, Ricardo M.; Engel, Matthias
Journal of Medicinal Chemistry, 2011 , vol. 54, # 19 p. 6714 - 6723
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-50°C; 12 h;
参考文献
Matsunaga, Hirokazu; Ikeda, Kiyoshi; Iwamoto, Ken-ichi; Suzuki, Yumiko; Sato, Masayuki
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2334 - 2336
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-40 - 20°C; 4.75 h;
参考文献
Matsunaga, Hirokazu; Ikeda, Kiyoshi; Iwamoto, Ken-ichi; Suzuki, Yumiko; Sato, Masayuki
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2334 - 2336
反应条件
1: KOH / H2O / 3 h / 80 °C 2: 65 percent / Ac2O / 130 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 12 p. 1938 - 1950
反应条件
1: piperidine / 20 °C 2: KOH / H2O / 3 h / 80 °C 3: 65 percent / Ac2O / 130 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 12 p. 1938 - 1950
参考文献
Ji, Lei; Ma, Yuheng; Li, Jin; Zhang, Liangren; Zhang, Lihe
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6166 - 6168
