3,6,9,12,15-五氧杂双环[15.3.1]二十一碳-1(21),17,19-三烯合成路线 （共 5 条）
反应条件
sodium hydride in tetrahydrofuran
20 h; Heating;
参考文献
Tuladhar, Sudersan M.; Williams, Gwyn; D'Silva, Claudius
Analytical Chemistry, 1991 , vol. 63, # 20 p. 2282 - 2285
反应条件
1: KH
2: 1.) Mg; 2.) D2O + H3O(+) / 1. THF, 7 day
View Scheme
参考文献
Markies,P.R.; Akkerman,Os.; Bickelhaupt,F.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4284
反应条件
1: Irradiation; bromination
2: KH
3: 1.) Mg; 2.) D2O + H3O(+) / 1. THF, 7 day
View Scheme
参考文献
Markies,P.R.; Akkerman,Os.; Bickelhaupt,F.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4284
反应条件
magnesium in tetrahydrofuran
168 h;
参考文献
Markies,P.R.; Akkerman,Os.; Bickelhaupt,F.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4284
反应条件
oxonium; water-d2; magnesium
1. THF, 7 day; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Markies,P.R.; Akkerman,Os.; Bickelhaupt,F.
Journal of the American Chemical Society, 1988 , vol. 110, p. 4284
