2,4,5,6-四氨基嘧啶硫酸盐合成路线 (共 25 条)
反应条件
triethylamine in water; N,N-dimethyl-formamide
T=20°C; 720 h;
参考文献
Zav'yalov, S. I.; Zavoshin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 419 - 422
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 452 - 455
反应条件
piperidine in water
T=20°C; 168 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1355 - 1357
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1666 - 1668
反应条件
piperidine in water
550 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1355 - 1357
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1666 - 1668
反应条件
piperidine in water
240 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zav'yalov, S. I.; Zavozin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1355 - 1357
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1666 - 1668
反应条件
sodium hydrogensulfite in water
T=80°C; 5.5 h; further cyclizating agents; Product distribution;
参考文献
Zav'yalov, S. I.; Zavoshin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 2 p. 419 - 422
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 2 p. 452 - 455