反应条件
1: 27 percent / LiAlH4 / tetrahydrofuran / 20 h / Heating
2: 60 percent / AlCl3, HCl / CH2Cl2 / 0.5 h / 0 °C
3: 1.) p-TsNHNH2, HCl, 2.) NaOMe / 1.) THF, reflux, 30 min, 2.) irradiation, 22 h
View Scheme
参考文献
Murad, Abo El-Fetouh El-Sayed; Hopf, Henning
Chemische Berichte, 1980 , vol. 113, # 7 p. 2358 - 2371
