4,7-二氯-1,10-菲咯啉合成路线 （共 9 条）
反应条件
trichlorophosphate 6 h; Heating;
参考文献
Molock, Frank F.; Boykin, David W.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 681 - 686
反应条件
1: 86 percent / diphenyl ether / 0.5 h / Heating 2: POCl3 / 2 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 16 p. 6190 - 6199
反应条件
1: 90 percent / paraffin / 1 h / 320 - 325 °C 2: 93 percent / phosphorus oxychloride / 6 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 681 - 686
反应条件
1: 85 percent / 10percent aq. KOH / Heating; overnight 2: 90 percent / paraffin / 1 h / 320 - 325 °C 3: 93 percent / phosphorus oxychloride / 6 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 681 - 686
反应条件
1.1: 2 h / Heating 1.2: 77 percent / Heating 2.1: 86 percent / diphenyl ether / 0.5 h / Heating 3.1: POCl3 / 2 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 16 p. 6190 - 6199
反应条件
trichlorophosphate 2 h; Heating;
参考文献
Organic Letters, , vol. 8, # 13 p. 2779 - 2782
反应条件
1: 90 percent / paraffin / 0.5 h / 245 °C 2: 85 percent / 10percent aq. KOH / Heating; overnight 3: 90 percent / paraffin / 1 h / 320 - 325 °C 4: 93 percent / phosphorus oxychloride / 6 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 681 - 686
反应条件
sodium methylate 1 h; Heating;
参考文献
Levis, Michael; Luening, Ulrich; Mueller, Michael; Schmittel, Michael; Woehrle, Clemens
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1994 , vol. 49, # 5 p. 675 - 682
反应条件
methanol; copper T=160°C;
参考文献
Zacharias; Case
Journal of Organic Chemistry, 1962 , vol. 27, p. 3878,3880
