2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 (共 203 条)
反应条件
toluene-4-sulfonic acid in deuterated toluene T=70 - 90°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 49, # 26 p. 5102 - 5105
反应条件
Aliquatreg; 336 in toluene T=70°C; 6 h;
参考文献
Dehmlow, Eckehard V.; Shamout, Abdul Rahman
Liebigs Annalen der Chemie, 1982 , # 9 p. 1753 - 1755
反应条件
pyridine; acetone; anhydrous zinc sulfate
参考文献
Zhurnal Obshchei Khimii, , vol. 24, p. 239
Chem.Abstr., , p. 4525
反应条件
1: 48 percent / 600 °C / 0.1 - 1 Torr 2: p-TsOH / toluene-d8 / 1 h / 70 - 90 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 26 p. 5102 - 5105
反应条件
1: 48 percent / 600 °C / 0.1 - 1 Torr 2: p-TsOH / toluene-d8 / 1 h / 70 - 90 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 26 p. 5102 - 5105
参考文献
Bell, Kelcey; Sadasivam, Dhandapani V.; Gudipati, Indra Reddy; Ji, Hua; Birney, David
Tetrahedron Letters, 2009 , vol. 50, # 12 p. 1295 - 1297
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile; potassium carbonate 1) -78 deg C, 2) -78 to 0 deg C, 2) 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 22 p. 6000 - 6002
反应条件
in xylene T=91.7°C; 0.75 h; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 111, # 6 p. 2186 - 2193
反应条件
diethyl ether; acetone; zinc(II) chloride
参考文献
Journal of the Chemical Society, , p. 244
参考文献
Journal of Organic Chemistry, , vol. 21, p. 821
Journal of the American Chemical Society, , vol. 75, p. 5400
Journal of the American Chemical Society, , vol. 77, p. 6641
Journal of the American Chemical Society, , vol. 78, p. 6421