2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 （共 203 条）
反应条件
in xylene
T=91.7°C; various temperatures, concentrations, mol ratio; Rate constantMechanismThermodynamic data;
参考文献
Clemens, Robert J.; Witzeman, Stewart J.
Journal of the American Chemical Society, 1989 , vol. 111, # 6 p. 2186 - 2193
反应条件
triethylamine in 1,4-dioxane
15 h; Heating;
参考文献
Boehme, Thomas M.; Augelli-Szafran, Corinne E.; Hallak, Hussein; Pugsley, Thomas; Serpa, Kevin; Schwarz, Roy D.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 14 p. 3094 - 3102
反应条件
in toluene
T=110°C; 0.3 h; Inert atmosphere;
参考文献
Chikhalikar, Sandip; Bhawe, Vijay; Jachak, Madhukar; Ghagare, Maruti
European Journal of Organic Chemistry, 2011 , # 30 p. 6085 - 6091
反应条件
in neat (no solvent)
T=130°C; 0.5 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Heterocycles, 1982 , vol. 17, p. 297 - 300
反应条件
in neat (no solvent)
T=131 - 132°C; 0.166667 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
反应条件
T=130°C; 0.133333 h;
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Heterocycles, 1982 , vol. 17, p. 297 - 300
反应条件
in neat (no solvent)
T=130 - 135°C; 0.166667 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
反应条件
T=130°C; 0.166667 h;
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Heterocycles, 1982 , vol. 17, p. 297 - 300
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
1 h; Heatingirradiation;
参考文献
Wolfe; Ro; Shi
Canadian Journal of Chemistry, 2001 , vol. 79, # 8 p. 1259 - 1271
