2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 (共 203 条)
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran
T=-78°C;
2: With 1,2,2-trichloro-1,1,2-trichloro-ethane in tetrahydrofuran
T=-50°C;
参考文献
Simpson, Thomas J.; Soulas, Florilene; Willis, Christine L.
Synlett, 2008 , # 14 p. 2196 - 2198
反应条件
in xylene
0.5 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
T=120 - 130°C; 0.5 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
in xylene
0.5 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
in xylene
0.5 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
N,N-dimethyl-aniline
T=120 - 130°C; 0.333333 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
T=120°C; 0.5 h; Heatingwith aliphatic and aromatic amides; also refluxing in xylene; new method to prepare N-acylacetoacetamides; Product distributionMechanism;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
T=120 - 130°C; 0.5 h; Heating;
参考文献
Sato, Masayuki; Kanuma, Norio; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1315 - 1321
反应条件
in dichloromethane
T=400°C; Cycloaddition; P=0.25 Torr; Thermolysis;
参考文献
Shumway; Ham; Moer; Whittlesey; Birney
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7731 - 7739