2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 （共 203 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide in tetrahydrofuran
T=-78 - 25°C;
参考文献
Winkler, Jeffrey D.; McLaughlin, Emily C.
Organic Letters, 2005 , vol. 7, # 2 p. 227 - 229
反应条件
in xylene
1 h; Heating;
参考文献
Doyle, Michael P.; Dyatkin, Alexey B.
Journal of Organic Chemistry, 1995 , vol. 60, # 10 p. 3035 - 3038
参考文献
Pourmorad; Hadizadeh; Shafiee
Pharmaceutical Sciences, 1997 , vol. 3, # 4 p. 165 - 168
反应条件
T=400°C; P=7.5006E-06 Torr;
参考文献
Audouard, Christophe; Bettaney, Kim; Doan, Chau T.; Rinaudo, Giuseppe; Jervis, Peter J.; Percy, Jonathan M.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 8 p. 1573 - 1582
反应条件
T=400°C; P=0.1 Torr;
参考文献
Freiermuth, Beat; Wentrup, Curt
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2286 - 2289
反应条件
pyrolysis at various conditions; Product distribution;
参考文献
Freiermuth, Beat; Wentrup, Curt
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2286 - 2289
反应条件
sodium acetate in tetrahydrofuran
24 h; Reflux;
参考文献
Sridharan, Vellaisamy; Ruiz, Miriam; Menendez, J. Carlos
Synthesis, 2010 , # 6 art. no. T12709SS, p. 1053 - 1057
反应条件
in neat (no solvent)
T=130 - 135°C; 0.583333 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
反应条件
in neat (no solvent)
T=130 - 135°C; 0.25 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
反应条件
in neat (no solvent)
T=120 - 121°C; 0.333333 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
