2,2,6-三甲基-4H-1,3-二英-4-酮合成路线 (共 203 条)
参考文献
Huggins, Michael T.; Barber, Patrick S.; Florian, David; Howton, William
Synthetic Communications, 2008 , vol. 38, # 23 p. 4226 - 4239
反应条件
N-bromosuccinmide; acetic acid T=20°C; 15 h; Darkness;
参考文献
Vieira, Adriano S.; Cunha, Rodrigo L.O.R.; Klitzke, Clecio F.; Zukerman-Schpector, Julio; Stefani, Helio A.
Tetrahedron, 2010 , vol. 66, # 3 p. 773 - 779
参考文献
Jaeger,G.; Wenzelburger,J.
Justus Liebigs Annalen der Chemie, 1976 , p. 1689 - 1712
反应条件
in anhydrous xylene T=120 - 150°C; Inert atmosphere;
参考文献
Chan, Wai-Wing; Kwong, Tsz-Lung; Yu, Wing-Yiu
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 18 p. 3749 - 3755
反应条件
in xylene T=140°C; 1.5 h;
参考文献
Sakaki; Kobayashi; Sato; Kaneko
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 11 p. 2952 - 2960
反应条件
in anhydrous xylene T=150°C; 2 h;
参考文献
Iman, Maryam; Davood, Asghar; Nematollahi, Ali Reza; Dehpoor, Ahmad Rerza; Shafiee, Abbas
Archives of Pharmacal Research, 2011 , vol. 34, # 9 p. 1417 - 1426
反应条件
sodium acetate in tetrahydrofuran 24 h; Reflux;
参考文献
Li, Suhua; Chen, Gang; Feng, Chen-Guo; Gong, Wei; Yu, Jin-Quan
Journal of the American Chemical Society, 2014 , vol. 136, # 14 p. 5267 - 5270
反应条件
T=120 - 130°C; 0.5 h; Heating;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 30, # 4 p. 1315 - 1321
反应条件
in toluene T=110°C; 0.0833333 h; Inert atmosphere;
参考文献
Chikhalikar, Sandip; Bhawe, Vijay; Jachak, Madhukar; Ghagare, Maruti
European Journal of Organic Chemistry, 2011 , # 30 p. 6085 - 6091
反应条件
in xylene T=150°C; 0.5 h; Product distribution;
参考文献
Clemens, Robert J.; Hyatt, John A.
Journal of Organic Chemistry, 1985 , vol. 50, # 14 p. 2431 - 2435