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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
53948-03-1
合成路线
（共 5 条）
13909-73-4
2′,3′,4′-三甲氧基苯乙酮
→
反应条件
53948-03-1
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / |Reflux; |Inert atmosphere 2: boron trifluoride diethyl etherate / 48 h / |Reflux 3: 3 h / 80 °C 4: iodine / methanol / 20 °C 5: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / |Reflux View Scheme
参考文献
Zaninetti, Roberta; Cortese, Salvatore V.; Aprile, Silvio; Massarotti, Alberto; Canonico, Pier Luigi; Sorba, Giovanni; Grosa, Giorgio; Genazzani, Armando A.; Pirali, Tracey
ChemMedChem, 2013 , vol. 8, # 4 p. 633 - 643
30225-96-8
→
反应条件
53948-03-1
反应条件
1: 3 h / 80 °C 2: iodine / methanol / 20 °C 3: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / |Reflux View Scheme
参考文献
Zaninetti, Roberta; Cortese, Salvatore V.; Aprile, Silvio; Massarotti, Alberto; Canonico, Pier Luigi; Sorba, Giovanni; Grosa, Giorgio; Genazzani, Armando A.; Pirali, Tracey
ChemMedChem, 2013 , vol. 8, # 4 p. 633 - 643
1453477-76-3
→
反应条件
53948-03-1
反应条件
1: iodine / methanol / 20 °C 2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / |Reflux View Scheme
参考文献
Zaninetti, Roberta; Cortese, Salvatore V.; Aprile, Silvio; Massarotti, Alberto; Canonico, Pier Luigi; Sorba, Giovanni; Grosa, Giorgio; Genazzani, Armando A.; Pirali, Tracey
ChemMedChem, 2013 , vol. 8, # 4 p. 633 - 643
30225-80-0
→
反应条件
53948-03-1
反应条件
1: boron trifluoride diethyl etherate / 48 h / |Reflux 2: 3 h / 80 °C 3: iodine / methanol / 20 °C 4: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / |Reflux View Scheme
参考文献
Zaninetti, Roberta; Cortese, Salvatore V.; Aprile, Silvio; Massarotti, Alberto; Canonico, Pier Luigi; Sorba, Giovanni; Grosa, Giorgio; Genazzani, Armando A.; Pirali, Tracey
ChemMedChem, 2013 , vol. 8, # 4 p. 633 - 643
1453477-74-1
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
53948-03-1
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran; water Suzuki Coupling; Reflux;
参考文献
Zaninetti, Roberta; Cortese, Salvatore V.; Aprile, Silvio; Massarotti, Alberto; Canonico, Pier Luigi; Sorba, Giovanni; Grosa, Giorgio; Genazzani, Armando A.; Pirali, Tracey
ChemMedChem, 2013 , vol. 8, # 4 p. 633 - 643
