2-乙基-1,3-二氧戊环-4-甲醇合成路线 （共 5 条）
反应条件
water; toluene-4-sulfonic acid T=0.85°C; Hydrolysis; Equilibrium constantActivation energy; Further Variations:Temperatures;
参考文献
Shevchuk; Podgornova; Piskaikina
Russian Journal of Applied Chemistry, 1999 , vol. 72, # 5 p. 853 - 856
反应条件
tris(triphenylphosphine)ruthenium(II) chloride
T=120°C; 1 h;
参考文献
Urbala, Magdalena; Kuznik, Nikodem; Krompiec, Stanislaw; Rzepa, Jozef
Synlett, 2004 , # 7 p. 1203 - 1206
反应条件
toluene-4-sulfonic acid in benzene
Heating; Title compound not separated from byproducts;
参考文献
Szeja, Wieslaw
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 609 - 612
参考文献
Trister; Hibbert
Canadian Journal of Research, Section B: Chemical Sciences, 1936 , vol. 14, p. 415,424
Full Text Show Details
Aksnes et al.
Acta Chemica Scandinavica (1947-1973), 1965 , vol. 19, p. 920,928,929
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; toluene-4-sulfonic acid
1.) benzene, reflux, 2.) benzene, from 0 deg C to 5 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Szeja, Wieslaw
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 609 - 612
