1,5-二苯基-3-戊酮合成路线 （共 80 条）
反应条件
potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Shim, Sang Chul
Journal of Organometallic Chemistry, 2006 , vol. 691, # 20 p. 4329 - 4332
反应条件
C69H123N6(3+)*3I(1-); hydrogen in tetrahydrofuran
T=20°C; P=2250.23 Torr; 18 h;
参考文献
Planellas, Marc; Pleixats, Roser; Shafir, Alexandr
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 651 - 662
反应条件
3-methyl-2-amino-pyridine; [RhCl(PPh3)2]; α,α,α-Trifluoro-p-toluic acid in toluene
T=110°C; 12 h;
参考文献
Jo, Eun-Ae; Jun, Chul-Ho
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3338 - 3340
反应条件
copper(l) iodide; potassium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in tetrahydrofuran
3 h; Reflux;
参考文献
Sun, Changhul; Fang, Yewen; Li, Shuang; Zhang, Yue; Zhao, Qlwu; Zhu, Shana; Li, Chaozhong
Organic Letters, 2009 , vol. 11, # 18 p. 4084 - 4087
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; potassium hydroxide in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
1: NaOH / ethanol; H2O
2: H2 / Pd-C / ethyl acetate
View Scheme
参考文献
Weber, Waylon M.; Hunsaker, Lucy A.; Abcouwer, Steve F.; Deck, Lorraine M.; Vander Jagt, David L.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 11 p. 3811 - 3820
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; dodec-1-ene; potassium hydroxide in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
[Pd(NCCH3)2(1,3-bis(diphenylphosphino)propane)](BF4)2; hydrogen
T=77°C; P=121600 Torr; 4 h; other cationic palladium(II)-diphosphine complexes; var. rection conditions; Product distributionMechanism;
参考文献
Pisano, Carmelina; Consiglio, Giambattista; Sironi, Angelo; Moret, Massimo
Journal of the Chemical Society, Chemical Communications, 1991 , # 6 p. 421 - 423
反应条件
Pd(O2CCF3)2lt;CH2(CH2PPh2)2gt; in methanol
T=100°C; P=15001.2 Torr; 4 h; Further byproducts given;
参考文献
Pisano, Carmelina; Consiglio, Giambattista
Gazzetta Chimica Italiana, 1994 , vol. 124, # 10 p. 393 - 402
反应条件
platinum
Hydrogenation;
参考文献
Nightingale; Wadsworth
Journal of the American Chemical Society, 1947 , vol. 69, p. 1181
Journal of the American Chemical Society, 1945 , vol. 67, p. 416
