1-(3-羟基-2-硝基苯基)乙酮合成路线 （共 9 条）
反应条件
1: 96 percent / H2 / Pt-C 2: 95 percent / Et3N / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Escobar, Carlos A.; Kluge, Michael; Sicker, Dieter
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 5 p. 1407 - 1414
反应条件
hydrogen; platinum on activated charcoal in tetrahydrofuran P=760 Torr; 5 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 34, # 5 p. 1407 - 1414
反应条件
potassium carbonate in dimethyl sulfoxide T=50°C; 20 h;
参考文献
Okuro, Kazumi; Gurnham, Joanna; Alper, Howard
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4715 - 4720
反应条件
potassium hydroxide 1.) r.t., 30 min, 2.) 30 min;
参考文献
Muller; Back
Archiv der Pharmazie, 1983 , vol. 316, # 8 p. 707 - 712
反应条件
sulfuric acid; nitric acid
T=-20°C; 0.416667 h;
参考文献
Fuerstner, Alois; Domostoj, Mathias M.; Scheiper, Bodo
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 8087 - 8094
反应条件
acetic acid; potassium nitrate
T=20 - 60°C;
参考文献
Guo, Wei; Liu, Wenfeng; Zhu, Lingjian; Zhang, Yongqiang; Cheng, Pengfei; Dong, Guoqiang; Zhuang, Chunlin; Yao, Jianzhong; Sheng, Chunquan; Miao, Zhenyuan; Zhang, Wannian
Chemistry and Biodiversity, 2011 , vol. 8, # 8 p. 1539 - 1549
反应条件
sulfuric acid; nitric acid
T=-20.1°C; 0.25 h;
参考文献
Cristiano, M. Lurdes S.; Johnstone, Robert A. W.; Pratt, Michael J.
Acta Crystallographica, Section C: Crystal Structure Communications, 1995 , vol. 51, # 12 p. 2581 - 2583
反应条件
pyridine hydrochloride
T=200°C;
参考文献
Spada; Casini
Gazzetta Chimica Italiana, 1950 , vol. 80, p. 642,647
反应条件
sulfuric acid; nitric acid
参考文献
Kluge; Sicker
Journal of Natural Products, 1998 , vol. 61, # 6 p. 821 - 822
