2-碘-3-硝基-苯甲酸合成路线 （共 24 条）
反应条件
hydrogenchloride; ethanol; tin(ll) chloride
参考文献
Stanley; McMahon; Adams
Journal of the American Chemical Society, 1933 , vol. 55, p. 706,712
反应条件
1: 4-methyl phenyl acetylene With ammonium hydroxide; copper(l) iodide in ethanol
0.25 h;
2: 2-iodo-3-nitrobenzoic acid With pyridine
Castro-Stephen coupling; 6 h; Heating;
参考文献
Woon, Esther C.Y.; Dhami, Archana; Mahon, Mary F.; Threadgill, Michael D.
Tetrahedron, 2006 , vol. 62, # 20 p. 4829 - 4837
反应条件
1: 4-ethynyl-1-methoxy-benzene With ammonium hydroxide; copper(l) iodide in ethanol
0.25 h;
2: 2-iodo-3-nitrobenzoic acid With pyridine
Castro-Stephen coupling; 6 h; Heating;
参考文献
Woon, Esther C.Y.; Dhami, Archana; Mahon, Mary F.; Threadgill, Michael D.
Tetrahedron, 2006 , vol. 62, # 20 p. 4829 - 4837
反应条件
thionyl chloride; N,N-dimethyl-formamide
24 h; Reflux;
参考文献
Dhami, Archana; Mahon, Mary F.; Lloyd, Matthew D.; Threadgill, Michael D.
Tetrahedron, 2009 , vol. 65, # 24 p. 4751 - 4765
