1: 78 percent / NaOMe / methanol; tetrahydrofuran / 17 h / -25 °C
2: 68 percent / xylene / 7 h / 140 °C
View Scheme
参考文献
Tichenor, Mark S.; Trzupek, John D.; Kastrinsky, David B.; Shiga, Futoshi; Hwang, Inkyu; Boger, Dale L.
Journal of the American Chemical Society, 2006 , vol. 128, # 49 p. 15683 - 15696
1.1: syn-benzaldehyde oxime; K2CO3 / dimethylformamide / 1.25 h / 90 °C
1.2: 86 percent / dimethylformamide / 2 h / 25 °C
2.1: 78 percent / NaOMe / methanol; tetrahydrofuran / 17 h / -25 °C
3.1: 68 percent / xylene / 7 h / 140 °C
View Scheme
参考文献
Tichenor, Mark S.; Trzupek, John D.; Kastrinsky, David B.; Shiga, Futoshi; Hwang, Inkyu; Boger, Dale L.
Journal of the American Chemical Society, 2006 , vol. 128, # 49 p. 15683 - 15696
1.1: syn-benzaldehyde oxime; K2CO3 / dimethylformamide / 1.25 h / 90 °C
1.2: 86 percent / dimethylformamide / 2 h / 25 °C
2.1: 78 percent / NaOMe / methanol; tetrahydrofuran / 17 h / -25 °C
3.1: 68 percent / xylene / 7 h / 140 °C
View Scheme
参考文献
Tichenor, Mark S.; Trzupek, John D.; Kastrinsky, David B.; Shiga, Futoshi; Hwang, Inkyu; Boger, Dale L.
Journal of the American Chemical Society, 2006 , vol. 128, # 49 p. 15683 - 15696
