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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯酚
合成路线
（共 365 条）
540-38-5
4-碘苯酚
→
反应条件
125151-59-9
反应条件
1: KOH / ethanol; H2O 2: triphenylphosphine; triethylamine / bis(triphenylphosphine) palladium dichloride; copper(I) iodide / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Yang, Yong Gang; Chen; Tang; Wen
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002 , vol. 373, p. 1 - 15
540-38-5
4-碘苯酚
→
反应条件
116130-33-7
2-氯-4-碘苯酚
反应条件
N,N-diisopropylmethyl amine; sulfuryl dichloride in toluene T=70°C; 1 h;
参考文献
PRESIDENT AND FELLOWS OF HARVARD COLLEGE; RITTER, Tobias; FURUYA, Takeru; TANG, Pingping
Patent: WO2010/59943 A2, 2010 ;
Location in patent: Page/Page column 77; 78 ;
540-38-5
4-碘苯酚
→
反应条件
119754-13-1
反应条件
1: 100 percent / PPTS / CH2Cl2 / 12 h / 20 °C 2: 80 percent / CuI; PPh3; NEt3 / (PPh3)2PdCl2 / 16 h / 65 °C View Scheme
参考文献
Sekine, Chizu; Fujisawa, Koichi; Iwakura, Kazunori; Minai, Masayoshi
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 364, p. 711 - 718
540-38-5
4-碘苯酚
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
1: potassium carbonate / acetone / 24 h / Reflux 2: copper / ethyl acetate / 2 h / 200 - 220 °C / Inert atmosphere View Scheme
参考文献
Sagrera, Gabriel; Bertucci, Ana; Vazquez, Alvaro; Seoane, Gustavo
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3060 - 3073
540-38-5
4-碘苯酚
→
反应条件
886-66-8
1,4-二苯基丁二炔
+
1849-26-9
反应条件
copper(l) iodide; [Pt(PPh3)4] in N,N-dimethyl-formamide T=120°C; 16 h;
参考文献
Synlett, , # 12 p. 2091 - 2094
540-38-5
4-碘苯酚
+
536-74-3
苯乙炔
→
反应条件
886-66-8
1,4-二苯基丁二炔
+
1849-26-9
反应条件
triethylamine; palladium complex immobilised on silica gel in various solvent(s) T=70°C; Sonogashira coupling; 12 h;
参考文献
Bandini, Marco; Luque, Rafael; Budarin, Vitaly; Macquarrie, Duncan J.
Tetrahedron, 2005 , vol. 61, # 41 p. 9860 - 9868
106-38-7
对溴甲苯
+
540-38-5
4-碘苯酚
+
98-80-6
苯硼酸
→
反应条件
644-08-6
4-甲基联苯
+
92-69-3
对苯基苯酚
反应条件
potassium carbonate in water T=20°C; Suzuki coupling; 97 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Safavi, Afsaneh; Motevalli, Somayeh; Doroodmand, Mohammad M.
Applied Organometallic Chemistry, 2012 , vol. 26, # 8 p. 417 - 424
540-38-5
4-碘苯酚
+
338945-22-5
→
反应条件
1257204-49-1
+
202925-92-6
反应条件
1: 4-hydroxyiodobenzene With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc in N,N-dimethyl-formamide T=0°C; Negishi coupling reaction; Inert atmosphere; 2: (S)-N-Boc-2-(iodomethyl)pyrrolidine in N,N-dimethyl-formamide T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
540-38-5
4-碘苯酚
→
反应条件
21784-73-6
+
89487-91-2
+
20294-48-8
反应条件
ammonium cerium(IV) nitrate in acetonitrile T=20°C; 2 h;
参考文献
Pan, Wen-Bin; Wei, Li-Mei; Wei, Li-Lan; Wu, Chin-Chung; Chang, Fang-Rong; Wu, Yang-Chang
Journal of the Chinese Chemical Society, 2005 , vol. 52, # 3 p. 581 - 588
540-38-5
4-碘苯酚
→
反应条件
20294-48-8
反应条件
iodine; silver nitrate in acetonitrile 2 h; Ambient temperature;
参考文献
Gaude, Didier; Gellon, Gisele; Goaller, Raymond Le; Pierre, Jean-Louis
Canadian Journal of Chemistry, 1989 , vol. 67, p. 104 - 108
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