5-甲基-1,3-二氢苯并咪唑-2-酮合成路线 (共 34 条)
反应条件
T=200°C; high vacuum sublimation;
参考文献
Branco; Prabhakar; Lobo; Williams
Tetrahedron, 1992 , vol. 48, # 30 p. 6335 - 6360
反应条件
dihydrogen peroxide in acetic anhydride
参考文献
Khalikov, S. S.; Molchanov, L. V.; Kadyrov, Ch. Sh.
Chemistry of Natural Compounds, 1983 , vol. 19, # 1 p. 124 - 125
Khimiya Prirodnykh Soedinenii, 1983 , # 1 p. 121
反应条件
T=750°C; P=0.05 - 0.07 Torr;
参考文献
Harvey, Ian W.; McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 681 - 690
反应条件
1: sodium borohydride / palladium charcoal (5percent) / pyridine / 0.25 h / 35 - 40 °C 2: 39 percent / 750 °C / 0.05 - 0.07 Torr View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 681 - 690
反应条件
in N,N-dimethyl acetamide 0.133333 h; Irradiation;
参考文献
Khajavi, Mohammad S.; Hajihadi, Mostafa; Nikpour, Farzad
Journal of Chemical Research - Part S, 1996 , # 2 p. 94 - 95
反应条件
in N,N-dimethyl acetamide 0.15 h; Irradiation;
参考文献
Khajavi, Mohammad S.; Hajihadi, Mostafa; Nikpour, Farzad
Journal of Chemical Research - Part S, 1996 , # 2 p. 94 - 95
反应条件
in N,N-dimethyl acetamide 0.0666667 h; Irradiation;
参考文献
Khajavi, Mohammad S.; Hajihadi, Mostafa; Nikpour, Farzad
Journal of Chemical Research - Part S, 1996 , # 2 p. 94 - 95
反应条件
in N,N-dimethyl acetamide 0.0666667 h; Irradiation;
参考文献
Khajavi, Mohammad S.; Hajihadi, Mostafa; Nikpour, Farzad
Journal of Chemical Research - Part S, 1996 , # 2 p. 94 - 95
反应条件
1: 67 percent / aq. sulphuric acid / acetic acid / 2.5 h / 100 °C 2: 83 percent / HCl / Heating 3: 46 percent / sodium ethoxide / ethanol; dimethylformamide / 2 h 4: 85 percent / cc. HCl / 4 h 5: 72 percent / aq.NH3 6: 39 percent / 750 °C / 0.05 - 0.07 Torr View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 681 - 690
反应条件
1: 72 percent / CH2Cl2 / 2 h / Ambient temperature 2: 82 percent / Et3N / acetonitrile; tetrahydrofuran / -35 °C 3: 93 percent / 200 °C / high vacuum sublimation View Scheme
参考文献
Tetrahedron, , vol. 48, # 30 p. 6335 - 6360