1-(3-硝基苯基)乙醇合成路线 (共 20 条)
反应条件
1: aq. HBr / acetic acid 2: ethanol 3: aq. H2SO4 4: H2 / Raney-Ni / ethanol 5: KICl2, aq. HCl 6: (i) H2SO4, (ii) aq. NaOH 7: aq. KOH / acetone View Scheme
参考文献
Felder; Pitre; Fumagalli; Lorenzotti
Journal of medicinal chemistry, 1970 , vol. 13, # 3 p. 559 - 561
反应条件
1: SOCl2 / CHCl3 2: AgNO3 / acetonitrile View Scheme
参考文献
Kochergin,P.M. et al.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 10 p. 2157 - 2161,2238 - 2242
反应条件
modified o-iodoxybenzoic acid in tetrahydrofuran; water T=60°C; 3 h;
参考文献
Thottumkara, Arun P; Vinod, Thottumkara K
Tetrahedron Letters, 2002 , vol. 43, # 4 p. 569 - 572
反应条件
Arthrobacter atrocyaneus in aq. phosphate buffer T=32°C; 72 h; Microbiological reaction; enantioselective reaction;
参考文献
Silva, Camila R.; Souza, Juliana C.; Araujo, Lidiane S.; Kagohara, Edna; Garcia, Thais P.; Pelizzari, Vivian H.; Andrade, Leandro H.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 23 - 28
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C 2: iodine / neat (no solvent) / 2 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
in water Irradiation; Quantum yield;
参考文献
Peter, Wan; Yates, Keith
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2076 - 2086
反应条件
tetrachloromethane; triphenylphosphine in chloroform 90 h;
参考文献
Hasan, Tayyaba; Sims, Leslie B.; Fry, Arthur
Journal of the American Chemical Society, 1983 , vol. 105, # 12 p. 3967 - 3975
反应条件
ammonium formate; PdMCM-41 in methanol T=69.84°C; 0.75 h;
参考文献
Selvam, Parasuraman; Sonavane, Sachin U.; Mohapatra, Susanta K.; Jayaram, Radha V.
Tetrahedron Letters, 2004 , vol. 45, # 15 p. 3071 - 3075
参考文献
Marvel; Overberger
Journal of the American Chemical Society, 1946 , vol. 68, p. 185
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C
2: iodine / neat (no solvent) / 2 h / 85 °C
View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999