反应条件
1.1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 20 °C / |Inert atmosphere; |Schlenk technique
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / |Inert atmosphere; |Schlenk technique
2.2: 1 h / -78 - 20 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Nitsch, Dominik; Huber, Stefan M.; Poethig, Alexander; Narayanan, Arjun; Olah, George A.; Prakash, G. K. Surya; Bach, Thorsten
Journal of the American Chemical Society, 2014 , vol. 136, # 7 p. 2851 - 2857