in neat (no solvent)
heating at 120°C, 6 hours;; vacuum distillation;;
参考文献
Bochkarev, M. N.; Maiorova, L. P.; Korneva, S. P.; Bochkarev, L. N.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1974 , vol. 73, p. 220 - 236
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.4, 4.2.1, page 165 - 169
in neat (no solvent)
byproducts: C2H6; under Ar, mixt. of ethyl(bis(pentafluorophenyl)germyl)thallium(I) and (C6F5)2GeH2 heated for 1 h at 100°C; soln. decanted from thallium, unreacted (C6F5)2GeH2 distilled in vac., residue sublimed at 140°C/0.1 mmHg;
参考文献
Bochkarev, M.N.; Basalgina, T.A.; Kalinina, G.S.; Razuvaev, G. A.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 405 - 410
