1-甲基-1H-吡唑并[3,4-d]嘧啶-4,6(5H,7H)-二酮合成路线 (共 7 条)
反应条件
phosphorus pentachloride; trichlorophosphate T=100°C; 12 h;
参考文献
PROGENICS PHARMACEUTICALS, INC.; HAN, Amy, Qi; WANG, Eric; GAUSS, Carla; XIE, Walter; COBURN, Glen; DEMUYS, Jean-Marc
Patent: WO2010/118367 A2, 2010 ;
Location in patent: Page/Page column 94 ;
反应条件
1: PCl5; POCl3 2: ethanol View Scheme
参考文献
Cheng; Robins
Journal of Organic Chemistry, 1958 , vol. 23, p. 852,855
Journal of Organic Chemistry, 1959 , vol. 24, p. 1570
反应条件
pyridine; tetraphosphorus decasulfide
参考文献
Cheng; Robins
Journal of Organic Chemistry, 1958 , vol. 23, p. 852,855
Journal of Organic Chemistry, 1959 , vol. 24, p. 1570
参考文献
Schmidt et al.
Helvetica Chimica Acta, 1958 , vol. 41, p. 1052,1056
Helvetica Chimica Acta, 1959 , vol. 42, p. 349,354
反应条件
1: PCl5; POCl3
2: ethanol; NH3
View Scheme
参考文献
Cheng; Robins
Journal of Organic Chemistry, 1958 , vol. 23, p. 852,855
Journal of Organic Chemistry, 1959 , vol. 24, p. 1570
反应条件
1: PCl5; POCl3
2: ethanol; NH3
View Scheme
参考文献
Cheng; Robins
Journal of Organic Chemistry, 1958 , vol. 23, p. 852,855
Journal of Organic Chemistry, 1959 , vol. 24, p. 1570
反应条件
1: PCl5; POCl3
View Scheme
参考文献
Cheng; Robins
Journal of Organic Chemistry, 1958 , vol. 23, p. 852,855
Journal of Organic Chemistry, 1959 , vol. 24, p. 1570