2-[1-(烯丙氧基)环丙基]乙酰胺合成路线 (共 2 条)
反应条件
1: With 1,1'-carbonyldiimidazole in tetrahydrofuran
T=25°C; 2.5 h;
2: With ammonium acetate in tetrahydrofuran
T=20°C; 16 h;
参考文献
Belov, Vladimir N.; Savchenko, Andrei I.; Sokolov, Viktor V.; Straub, Alexander; De Meijere, Armin
European Journal of Organic Chemistry, 2003 , # 3 p. 551 - 561
反应条件
1.1: 86 percent / NaH / kerosene / 0 °C
2.1: N,N'-carbonydiimidazole / tetrahydrofuran / 2.5 h / 25 °C
2.2: 74 percent / NH4OAc / tetrahydrofuran / 16 h / 20 °C
View Scheme
参考文献
Belov, Vladimir N.; Savchenko, Andrei I.; Sokolov, Viktor V.; Straub, Alexander; De Meijere, Armin
European Journal of Organic Chemistry, 2003 , # 3 p. 551 - 561