2-硝基-4-硫氰基苯胺合成路线 （共 28 条）
反应条件
potassium hydroxide in ethanol
参考文献
May and Baker Limited
Patent: US4034107 A1, 1977 ;
反应条件
1.1: sodium hydroxide / water; propan-1-ol / 35 °C / Industry scale 2.1: water; propan-1-ol / 40 - 60 °C / Industry scale 2.2: 60 °C 3.1: NaSH / methanol / 50 - 70 °C / Industry scale 4.1: hydrogenchloride / water; acetone / 80 - 85 °C / Industry scale 4.2: 20 - 85 °C / pH 4 - 4.5 View Scheme
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Naithani, Sushil; Natikar, Rajendra Devendra; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303782 A1, 2013 ;
反应条件
1.1: sodium hydroxide / water; propan-1-ol / 35 °C / Industry scale 2.1: water; propan-1-ol / 40 - 60 °C / Industry scale 2.2: 60 °C 3.1: NaSH / methanol / 50 - 70 °C / Industry scale View Scheme
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Naithani, Sushil; Natikar, Rajendra Devendra; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303782 A1, 2013 ;
反应条件
sodium hydroxide; PEG 400 in water T=75 - 100°C;
参考文献
Pilyugin; Chikisheva; Valitov; Sapozhnikov
Russian Journal of General Chemistry, 2002 , vol. 72, # 9 p. 1439 - 1443
反应条件
PEG-400; sodium hydroxide in water T=93 - 95°C; 5 h;
参考文献
Pilyugin; Sapozhnikov; Shitov
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 7 p. 979 - 984
反应条件
PEG-400; sodium hydroxide in water T=93 - 95°C; 5 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 39, # 7 p. 979 - 984
反应条件
PEG-400; sodium hydroxide in water T=93 - 95°C; 5 h;
参考文献
Pilyugin; Sapozhnikov; Shitov
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 7 p. 979 - 984
反应条件
1: 68 percent / aq. KOH / ethanol / 0.5 h / 20 °C
2: 74 percent / aq. Na2S2O4 / ethanol / 1 h / Heating
View Scheme
参考文献
Schmidt, Andreas; Gholipour Shilabin, Abbas; Nieger, Martin
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 23 p. 4342 - 4350
反应条件
sodium borohydride in N-methyl-acetamide
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4076825 A1, 1978 ;
参考文献
Challenger; Peters
Journal of the Chemical Society, 1928 , p. 1370
