2-硝基-4-硫氰基苯胺合成路线 （共 28 条）
反应条件
Alkaline hydrolysis;
参考文献
Pilyugin; Sapozhnikov; Shitov
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 7 p. 979 - 984
参考文献
Challenger; Peters
Journal of the Chemical Society, 1928 , p. 1370
反应条件
potassium hydroxide in ethanol
T=20°C; 0.5 h;
参考文献
Schmidt, Andreas; Gholipour Shilabin, Abbas; Nieger, Martin
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 23 p. 4342 - 4350
反应条件
sodium borohydride in N-methyl-acetamide; acetone
参考文献
Syntex (U.S.A.) Inc.
Patent: US4011320 A1, 1977 ;
反应条件
water; sodium hydroxide in propan-1-ol
T=35 - 60°C; Large scale;
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Naithani, Sushil; Natikar, Rajendra Devendra; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303782 A1, 2013 ;
Location in patent: Paragraph 0022 ;
反应条件
sodium borohydride in dichloromethane; acetonitrile
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4076825 A1, 1978 ;
反应条件
sodium cyanide; tri-n-butylmethylammonium chloride in propan-1-ol; dichloromethane; water
参考文献
Hernandez-Luis, Francisco; Castillo, Rafael; Yepez-Mulia, Lilian; Cedillo-Rivera, Roberto; Martinez-Vazquez, Gabriel; Morales-Hurtado, Raul; Jung, Helgi; Sanchez, Monica; Hernandez-Campos, Alicia; Viveros, Noemi; Munoz, Onofre
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 18 p. 2231 - 2236
反应条件
sodium borohydride in N-methyl-acetamide
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4145433 A1, 1979 ;
