2-(4-溴苯基)-4-苯基喹唑啉合成路线 （共 7 条）
反应条件
tert.-butylhydroperoxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
T=90 - 95°C; 9.5 h;
参考文献
Rachakonda, Sridhar; Pratap, P.Surya; Basaveswara Rao, Mandava V.
Synthesis (Germany), 2012 , vol. 44, # 13 art. no. SS-2012-Z0001-OP, p. 2065 - 2069
反应条件
1: phenyl-magnesium bromide; 2-amino-benzonitrile in tetrahydrofuran; diethyl ether
T=45°C; 2 h; Heating / reflux;
2: 4-bromo-benzoyl chloride in tetrahydrofuran; diethyl ether
T=0 - 45°C; 2.16 h; Heating / reflux;
3: With ammonium chloride in tetrahydrofuran; diethyl ether; water
T=0°C;
参考文献
IDEMITSU KOSAN COMPANY LIMITED
Patent: EP1808433 A1, 2007 ;
Location in patent: Page/Page column 21-22 ;
反应条件
1: phenyl-magnesium bromide; 2-amino-benzonitrile in tetrahydrofuran; diethyl ether
T=45°C; 2 h;
2: 4-bromo-benzoyl chloride in tetrahydrofuran; diethyl ether
T=0 - 45°C; 2.16667 h;
参考文献
Idemitsu Kosan Co., Ltd.
Patent: EP2415769 A1, 2012 ;
Location in patent: Page/Page column 120-121 ;
反应条件
α-D-Glcp-(1→4)-D-Glcp; N,N'-dimethyl-urea; ammonium acetate; ammonium chloride
T=90°C; 4.16667 h;
参考文献
Zhang, Zhan-Hui; Zhang, Xiao-Nan; Mo, Li-Ping; Li, Yong-Xiao; Ma, Fei-Ping
Green Chemistry, 2012 , vol. 14, # 5 p. 1502 - 1506
反应条件
1: bromobenzene With magnesium in tetrahydrofuran
2: 2-amino-benzonitrile in tetrahydrofuran
T=45°C; 2 h;
3: 4-bromo-benzoyl chloride in tetrahydrofuran; diethyl ether
T=0 - 45°C; 2.16667 h;
参考文献
Liu, Dong; Zhang, Zhenyu; Zhang, Hongyu; Wang, Yue
Chemical Communications, 2013 , vol. 49, # 85 p. 10001 - 10003
反应条件
1: CHCl3
2: 81 percent / acetic anhydride / 6 h / Heating
View Scheme
参考文献
Szczepankiewicz, Wojciech; Wagner, Pawel; Danicki, Miroslaw; Suwinski, Jerzy
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2015 - 2017
反应条件
1: CHCl3
2: 81 percent / acetic anhydride / 6 h / Heating
View Scheme
参考文献
Szczepankiewicz, Wojciech; Wagner, Pawel; Danicki, Miroslaw; Suwinski, Jerzy
Tetrahedron Letters, 2003 , vol. 44, # 10 p. 2015 - 2017
