3-(4-甲氧苯基)-1-丙醇合成路线 (共 74 条)
反应条件
1: H2 / 10 percent Pd/C / tetrahydrofuran / 2068.59 Torr 2: LiAlH4 / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 45, # 16 p. 3549 - 3557
反应条件
C15H22Cl2N3O2PRu; glycerol; potassium hydroxide T=100°C; 6 h; Inert atmosphere;
参考文献
Diaz-Alvarez, Alba E.; Crochet, Pascale; Cadierno, Victorio
Catalysis Communications, 2011 , vol. 13, # 1 p. 91 - 96
反应条件
sodium tetrahydroborate in tetrahydrofuran 1) 0 deg C, 2 h, 2) rt, 2 h;
参考文献
Kasturi; Pragnacharyulu
Tetrahedron, 1992 , vol. 48, # 21 p. 4431 - 4438
反应条件
4-(N,N-dimethlyamino)pyridine; formic acid; Rh6(CO)12; carbon monoxide in tetrahydrofuran T=30°C; P=3800 Torr; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 7 p. 2378 - 2381
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; Hydrolysis;
参考文献
Organic Letters, , vol. 2, # 10 p. 1455 - 1456
反应条件
potassium hydroxide; isopropyl alcohol; PdMCM-41 5 h;
参考文献
Selvam, Parasuraman; Sonavane, Sachin U.; Mohapatra, Susanta K.; Jayaram, Radha V.
Tetrahedron Letters, 2004 , vol. 45, # 15 p. 3071 - 3075
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Heating;
参考文献
Tetrahedron Letters, , vol. 34, # 14 p. 2343 - 2346
参考文献
E. R. Squibb and Sons, Inc.
Patent: US5100889 A1, 1992 ;
反应条件
potassium fluoride; 3-chloro-benzenecarboperoxoic acid in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Palframan, Matthew J.; Parsons, Andrew F.; Johnson, Paul
Synlett, 2011 , # 19 art. no. D28811ST, p. 2811 - 2814
反应条件
sodium tetrahydroborate; zwitterionic rhodium ν6-tetraphenylborate; isopropyl alcohol in chloroform T=100°C; P=25857.4 Torr; 22 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 4 p. 233 - 234