3-(4-甲氧苯基)-1-丙醇合成路线 (共 74 条)
反应条件
tetrachloromethane; triphenylphosphine 8 h; Heating;
参考文献
Fronza, Giovanni; Fuganti, Claudio; Serra, Stefano; Cisero, Marco; Koziet, Joseph
Journal of agricultural and food chemistry, 2002 , vol. 50, # 10 p. 2748 - 2754
反应条件
1: 98 percent / DMSO; oxalyl chloride; Et3N / CH2Cl2 / -78 - 0 °C 2: 94 percent / TiCl4*2THF; Zn / tetrahydrofuran / 4 h / Heating 3: aq. LiOH / tetrahydrofuran; methanol / 96 h / 20 °C View Scheme
参考文献
Xiao, Xiangshu; Antony, Smitha; Kohlhagen, Glenda; Pommier, Yves; Cushman, Mark
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7495 - 7501
反应条件
oxalyl dichloride; triethylamine in dichloromethane; dimethyl sulfoxide T=-78°C; Swern oxidation; 0.5 h; Inert atmosphere;
参考文献
Bercovici, Daniel A.; Brewer, Matthias
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9890 - 9893
反应条件
iodine; potassium carbonate in toluene Reflux;
参考文献
Choudhary, Vasant R.; Dumbre, Deepa K.
Catalysis Communications, 2011 , vol. 13, # 1 p. 82 - 86
反应条件
n-butyllithium 2.) ether, hexane, room temperature, 12 h; Yield given. Multistep reaction;
参考文献
Yoshizawa, Yuko; Kawaii, Satoru; Kanauchi, Masatoshi; Chida, Manami; Mizutani, Junya
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 9 p. 1572 - 1574
反应条件
1: in dichloromethane cooling; 2: With dibenzyl azodicarboxylate in dichloromethane cooling; 3: With trifluoroacetic acid in dichloromethane Further stages.;
参考文献
Sun, Weilin; Pelletier, Jeffrey C.
Tetrahedron Letters, 2007 , vol. 48, # 44 p. 7745 - 7746
反应条件
hydrogen bromide; acetic acid
参考文献
Takei; Sakato; Ono
Bl. Inst. phys. chem. Res. Abstr. Tokyo, 1938 , vol. 11, p. 6
Chem. Zentralbl., 1939 , vol. 110, # I p. 1183
Full Text Show Details
Takei; Sakato; Ono
Rikagaku Kenkyusho Iho, 1938 , vol. 17, p. 216,225
Bl.Inst.phys.chem.Res.Abstr.Tokyo, 1938 , vol. 11, p. 6
Chem. Zentralbl., 1939 , vol. 110, # I p. 1183
反应条件
pyridine Leiten des Reaktionsprodukts ueber Glas bei 400grad;
参考文献
Fort; Roberts
Journal of the American Chemical Society, 1956 , vol. 78, p. 584,589
反应条件
iodine; potassium carbonate 80 h; Heating;
参考文献
Mori, Naoshi; Togo, Hideo
Tetrahedron, 2005 , vol. 61, # 24 p. 5915 - 5925
反应条件
ammonium hydroxide; iodine T=60°C; 21 h;
参考文献
Iida, Shinpei; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 34 p. 8274 - 8281