2,2'-(甲基亚胺)二乙醇盐酸盐合成路线 （共 3 条）
反应条件
thionyl chloride in chloroform Chlorination; 2 h; Heating;
参考文献
Friebe, Matthias; Mahmood, Ashfaq; Spies, Hartmut; Berger, Ralf; Johannsen, Bernd; Mohammed, Ashour; Eisenhut, Michael; Bolzati, Cristina; Davison, Alan; Jones, Alun G.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 14 p. 2745 - 2752
反应条件
1: 99 percent / thionyl chloride / CHCl3 / 2 h / Heating 2: 88 percent / ethanol / 5 h / Heating 3: 45 percent / aq. NaOH / 0.08 h / 100 °C View Scheme
参考文献
Friebe, Matthias; Mahmood, Ashfaq; Spies, Hartmut; Berger, Ralf; Johannsen, Bernd; Mohammed, Ashour; Eisenhut, Michael; Bolzati, Cristina; Davison, Alan; Jones, Alun G.
Journal of Medicinal Chemistry, 2000 , vol. 43, # 14 p. 2745 - 2752
反应条件
hydrogenchloride in ethanol; water
T=24.99°C; P=757.576 Torr; 12 h;
参考文献
Zhao, Yansong; Zhang, Xiangping; Zeng, Shaojuan; Zhou, Qing; Dong, Haifeng; Tian, Xiao; Zhang, Suojiang
Journal of Chemical and Engineering Data, 2010 , vol. 55, # 9 p. 3513 - 3519
