1,4-联苯基-1-丁酮合成路线 （共 73 条）
反应条件
carbon disulfide; aluminium trichloride
参考文献
Borsche; Sinn
Justus Liebigs Annalen der Chemie, 1942 , vol. 553, p. 260,267
参考文献
Borsche; Sinn
Justus Liebigs Annalen der Chemie, 1942 , vol. 553, p. 260,267
反应条件
in acetone Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Forward, Philip; Hunter, William N.; Leonard, Gordon A.; Palou, Josefina; Walmsley, David; Watt, C. Ian F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 5 p. 931 - 935
反应条件
[IrH(1,5-cyclooctadiene)Cl(HCN(i-Pr)CHCN(C2H4PPh2))]PF6; potassium hydroxide in toluene
T=110°C; 1 h; Inert atmosphere;
参考文献
Gong, Xue; Zhang, Hong; Li, Xingwei
Tetrahedron Letters, 2011 , vol. 52, # 43 p. 5596 - 5600
反应条件
[Li(tmeda)]2[Fe(C2H4)4] in tetrahydrofuran
T=-20°C;
参考文献
Martin, Ruben; Fuerstner, Alois
Angewandte Chemie - International Edition, 2004 , vol. 43, # 30 p. 3955 - 3957
反应条件
3-methyl-2-amino-pyridine; benzoic acid; Wilkinson's catalyst
T=140°C; 0.166667 h; Irradiation;
参考文献
Loupy, Andre; Chatti, Saber; Delamare, Sarah; Lee, Dae-Yon; Chung, Jong-Hwa; Jun, Chul-Ho
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1280 - 1285
反应条件
1: phenyl 3-iodopropyl ketone With [Fe(C2H4)4][Li(tmeda)]2 in tetrahydrofuran
T=-20°C;
2: Bromure de phenyl magnesium in tetrahydrofuran; diethyl ether
T=-20°C; 0.0833333 h; Further stages.;
参考文献
Fuerstner, Alois; Martin, Ruben; Krause, Helga; Seidel, Guenter; Goddard, Richard; Lehmann, Christian W.
Journal of the American Chemical Society, 2008 , vol. 130, # 27 p. 8773 - 8787
反应条件
P(t-Bu)2Me; tetrabutyl ammonium fluoride; palladium (II) bromide in tetrahydrofuran
T=20°C; Hiyama coupling; 14 h;
参考文献
Lee, Jae-Young; Fu, Gregory C.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5616 - 5617
反应条件
1,4-bis(dicyclohexylphosphino)butane*2HBF4; palladium diacetate; sodium t-butanolate in toluene
T=110°C; 14 h; Inert atmosphere;
参考文献
Ziadi, Asraa; Martin, Ruben
Organic Letters, 2012 , vol. 14, # 5 p. 1266 - 1269
反应条件
1: (3-phenylpropyl)triphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane
T=-15°C;
2: N-Methoxy-N-methyl-benzamide in tetrahydrofuran; hexane
T=-78 - 20°C; Wittig reaction;
3: With hydrogenchloride in tetrahydrofuran; diethyl ether; hexane
T=20°C;
参考文献
Murphy, John A.; Commeureuc, Aurelien G. J.; Snaddon, Thomas N.; McGuire, Thomas M.; Khan, Tanweer A.; Hisler, Kevin; Dewis, Mark L.; Carling, Robert
Organic Letters, 2005 , vol. 7, # 7 p. 1427 - 1429
