4,4'-二苯基-2-丁酮合成路线 (共 85 条)
反应条件
cerium(III) chloride in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 12 p. 4392 - 4398
反应条件
hydrogenchloride; tetrabutyl-ammonium chloride; palladium dichloride in dichloromethane 5 h; Ambient temperature;
参考文献
Cacchi, S.; Misiti, D.
Tetrahedron, 1981 , vol. 37, # 16 p. 2941 - 2946
反应条件
lithium chloride; palladium dichloride in acetic acid T=25°C; Addition; Michael reaction; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 73, # 9 p. 2149 - 2155
反应条件
1: phenyl-magnesium bromide With [3-[(1R,2R)-2-[[(E)-(3,5-di-tert-butyl-2-hydroxyphenyl)methylidene]amino]cyclohexyl]-1-isopropyl-4-phenyl-3H-imidazol-1-ylidene]copper(I) bromide in diethyl ether T=25°C; 0.25 h; Inert atmosphere; 2: 4-phenylbut-3-en-2-one in diethyl ether T=25°C; 1.16667 h; Inert atmosphere; 3: With hydrogenchloride; water in diethyl ether
参考文献
Simonovic, Stevan; Whitwood, Adrian C.; Clegg, William; Harrington, Ross W.; Hursthouse, Michael B.; Male, Louise; Douthwaite, Richard E.
European Journal of Inorganic Chemistry, 2009 , # 13 SPEC. ISS. p. 1786 - 1795
反应条件
lithium chloride; palladium dichloride in acetic acid T=25°C; Addition; Michael reaction; 20 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 73, # 9 p. 2149 - 2155
反应条件
chloroform; palladium diacetate; caesium carbonate; triphenylphosphine in toluene T=80°C; 24 h; Inert atmosphere;
参考文献
Yamamoto, Tetsuya; Iizuka, Michiko; Takenaka, Hiroto; Ohta, Tetsuo; Ito, Yoshihiko
Journal of Organometallic Chemistry, 2009 , vol. 694, # 9-10 p. 1325 - 1332
参考文献
Koltunov, Konstantin Yu.; Walspurger, Stephane; Sommer, Jean
Chemical Communications, 2004 , # 15 p. 1754 - 1755
反应条件
antimony trichloride in acetic acid T=25°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 4 p. 883 - 888
反应条件
[Pd(1,2-bis(diphenylphosphanyl)ethane)(PhCN)2](SbF6)2; water in tetrahydrofuran T=20°C; 23 h;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 24 p. 2768 - 2770
反应条件
1: With [2,2']bipyridinyl; sodium acetate; copper(l) chloride in o-xylene T=135°C; 2: With hydrogenchloride in o-xylene; water
参考文献
Liao, Yuan-Xi; Hu, Qiao-Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7602 - 7607