4,4'-二苯基-2-丁酮合成路线 (共 85 条)
反应条件
1: With iron(III) trifluoromethanesulfonate T=80°C; 3 h; Neat (no solvent); 2: With methanol; iron(III) trifluoromethanesulfonate T=90°C; Retro-Claisen condensation; 24 h; Neat (no solvent);
参考文献
Biswas, Srijit; Maiti, Sukhendu; Jana, Umasish
European Journal of Organic Chemistry, 2010 , # 15 p. 2861 - 2866
反应条件
bis(acetylacetonato) palladium; oxygen; copper(II) oxide in 1,4-dioxane; water T=80°C; P=760.051 Torr; 24 h; Reagent/catalystSolvent;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 26 p. 4295 - 4298
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 2 h; Further byproducts given;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 46, p. 121 - 130
反应条件
formic acid; triethylamine; [Pd(PPh3)2(OAc)2] in acetonitrile T=80°C; 6 h; var. vinyl ketones; var. aryl iodides; var. times; var. Pd catalysts; var. solvents; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 48, # 23 p. 4236 - 4240
反应条件
silver(I) acetate; palladium diacetate in acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Tanabe, Koichiro; Uemura, Sakae
Tetrahedron Letters, 1994 , vol. 35, # 8 p. 1275 - 1278
反应条件
palladium diacetate; acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-Ichi; Ohe, Kouichi; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 8 p. 2341 - 2348
反应条件
tetrabutylammomium bromide; sodium hydrogencarbonate; palladium dichloride T=120°C; Heck coupling; 36 h;
参考文献
Journal of Organometallic Chemistry, , vol. 634, # 2 p. 153 - 156
反应条件
silica gel supported sodium hydrogen sulfate in anhydrous dichloroethane T=60°C; 0.5 h;
参考文献
Synlett, , # 20 art. no. U06611ST, p. 2971 - 2976
反应条件
copper(l) iodide in pyridine T=0°C; 3 h; Yield given;
参考文献
Tetrahedron, , vol. 39, # 9 p. 1621 - 1626
反应条件
silver(I) acetate; palladium diacetate in acetic acid T=25°C; Substitution; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 73, # 9 p. 2149 - 2155