4,4'-二苯基-2-丁酮合成路线 (共 85 条)
反应条件
iron(III) trifluoromethanesulfonate; butan-1-ol T=120°C; Retro-Claisen condensation; 24 h; Neat (no solvent);
参考文献
European Journal of Organic Chemistry, , # 15 p. 2861 - 2866
反应条件
chlototrimethylsilane in diethyl ether 1) 0 deg C, 1h, 2) up to rt, 3) 5 h;
参考文献
Bergdahl, Mikael; Lindstedt, Eva-Lotte; Nilsson, Martin; Olsson, Thomas
Tetrahedron, 1988 , vol. 44, # 7 p. 2055 - 2062
反应条件
water T=220°C; 12 h; Autoclave;
参考文献
Tetrahedron Letters, , vol. 51, # 14 p. 1847 - 1851
反应条件
in diethyl ether T=0°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 28, p. 348 - 355
反应条件
1,4-diaza-bicyclo[2.2.2]octane in xylene 5 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 20 p. 2943 - 2949
反应条件
palladium diacetate; silver(I) acetate; antimony trichloride; acetic acid T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-Ichi; Ohe, Kouichi; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 8 p. 2341 - 2348
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 5 h / 20 °C / Inert atmosphere 2: [Rh(OH)(cycloocta-1,5-diene)]2; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl / 1,4-dioxane; water / 3 h / 20 - 60 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 19 p. 5314 - 5317
反应条件
sodium acetate; antimony trichloride; palladium diacetate in acetic acid T=25°C; various catalysts, Lewis acids, bases, temperatures, and reaction time; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 60, # 4 p. 883 - 888
反应条件
T=-10 - -8°C; 2.5 h;
参考文献
Rahman, M. T.; Saha, S. L.; Hansson, A.-T.
Journal of Organometallic Chemistry, 1980 , vol. 199, # 1 p. 9 - 14
参考文献
Warner-Lambert Company
Patent: US5278326 A1, 1994 ;