4,4'-二苯基-2-丁酮合成路线 (共 85 条)
反应条件
in diethyl ether T=0°C;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 40, # 6 p. 466 - 469
反应条件
triethylamine; trifluoroacetic acid; palladium on activated charcoal in N,N-dimethyl-formamide T=80°C; 4 h; other bases, catalysts, acids; Product distribution;
参考文献
Tetrahedron, , vol. 45, # 3 p. 813 - 828
反应条件
palladium diacetate; silver(I) acetate; antimony trichloride; acetic acid T=25°C; 24 h; other α,β-unsaturated ketones and aldehydes; var. arylantimony compounds; Product distributionMechanism;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 8 p. 2341 - 2348
反应条件
1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Reflux 2: InI3; trimethylsilyl iodide / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry Letters, , vol. 40, # 11 p. 1223 - 1225
反应条件
1: di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; sodium carbonate / toluene / 6 h / 100 °C / Inert atmosphere 2: C19H8O7Ru3; dimethylphenylsilane / 1,4-dioxane / 3 h / 50 °C / Inert atmosphere View Scheme
参考文献
Tetrahedron, , vol. 68, # 15 p. 3243 - 3252
反应条件
in diethyl ether T=20°C; 3 h;
参考文献
Bioorganic Chemistry, , vol. 33, # 4 p. 325 - 337
反应条件
in diethyl ether T=20°C; Rate constant;
参考文献
Acta Chemica Scandinavica, , vol. 45, # 9 p. 925 - 929
反应条件
trimethylsilyl iodide; hydrogen cation 1.) ether, 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 45, # 2 p. 535 - 544
反应条件
potassium hydroxide; ethanol
参考文献
Journal of the Chemical Society, , vol. 71, p. 676
参考文献
Bulletin de la Societe Chimique de France, , p. 811 - 815