1-(3-甲基苯基)-3-苯基-1-丙酮合成路线 （共 11 条）
反应条件
lithium tert-butylate in toluene
T=110°C; 12 h; Inert atmosphere;
参考文献
Liang, Yu-Feng; Zhou, Xin-Feng; Tang, Shi-Ya; Huang, Yao-Bing; Feng, Yi-Si; Xu, Hua-Jian
RSC Advances, 2013 , vol. 3, # 21 p. 7739 - 7742
反应条件
in tetrahydrofuran
T=20°C; 2 h; Cooling with ice;
参考文献
Gembus, Vincent; Furman, Christophe; Millet, Regis; Mansouri, Roxane; Chavatte, Philippe; Levacher, Vincent; Briere, Jean-Francois
European Journal of Medicinal Chemistry, 2012 , vol. 58, p. 396 - 404
反应条件
potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Shim, Sang Chul
Journal of Organometallic Chemistry, 2006 , vol. 691, # 20 p. 4329 - 4332
反应条件
pyrrolidine; CataCXium POMetB; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl acetamide
T=140°C; 4 h; Inert atmosphereMolecular sieve;
参考文献
Colbon, Paul; Ruan, Jiwu; Purdie, Mark; Xiao, Jianliang
Organic Letters, 2010 , vol. 12, # 16 p. 3670 - 3673
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; potassium hydroxide in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; dodec-1-ene; potassium hydroxide in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II); potassium carbonate; butan-1-ol
0.5 h; Reflux; chemoselective reaction;
参考文献
Ding, Boqiang; Zhang, Zhenfeng; Liu, Yangang; Sugiya, Masashi; Imamoto, Tsuneo; Zhang, Wanbin
Organic Letters, 2013 , vol. 15, # 14 p. 3690 - 3693
反应条件
Iron(II,III) oxide nanopowder
T=280°C; dowtherm AInert atmosphere;
参考文献
Goossen, Lukas J.; Mamone, Patrizia; Oppel, Christoph
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 1 p. 57 - 63
反应条件
1: methanol; sodium tetrahydroborate
2: tris(triphenylphosphine)ruthenium(II) chloride; dodec-1-ene; potassium hydroxide / 1,4-dioxane / 40 h / 80 °C
View Scheme
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
1.1: 1,1'-carbonyldiimidazole / dichloromethane / 0.5 h / 0 °C
1.2: 0 - 20 °C
2.1: tetrahydrofuran / 2 h / 20 °C / |Cooling with ice
View Scheme
参考文献
Gembus, Vincent; Furman, Christophe; Millet, Regis; Mansouri, Roxane; Chavatte, Philippe; Levacher, Vincent; Briere, Jean-Francois
European Journal of Medicinal Chemistry, 2012 , vol. 58, p. 396 - 404
