water in water; toluene; butan-1-ol (CH3)2SiCl2 and SiCl4 (5:1 mol) in butanol-H2O-toluene; heating of the oily product at 350-600°C in a slow stream of N2;; fractional distn.; crystn. on cooling; recrystn. from toluene;;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 356 - 358
gallium triiodide T=175 - 180°C; 3 h; Yield givenFurther byproducts given. Title compound not separated from byproducts;
参考文献
Voronkov, M. G.; Tsyrendorzhieva, I. P.; Albanov, A. I.; Shergina, N. I.; Klyba, L. V.; Dubinskaya, E. I.
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 656 - 657
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 4 p. 697 - 698
