1-(4-甲基苯基)吡咯烷合成路线 （共 17 条）
反应条件
palladium 10 on activated carbon; sodium t-butanolate; 2-dicyclohexylphosphino-1,1'-biphenyl in tert-butyl alcohol
T=80°C; Buchwald-Hartwig amination; Inert atmosphere;
参考文献
Nasir Baig; Varma, Rajender S.
RSC Advances, 2014 , vol. 4, # 13 p. 6568 - 6572
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=120°C; 12 h;
参考文献
Heo, Yumi; Hyun, Dajung; Kumar, Manian Rajesh; Jung, Hyun Min; Lee, Sunwoo
Tetrahedron Letters, 2012 , vol. 53, # 49 p. 6657 - 6661
反应条件
potassium carbonate in ethanol; water
T=120°C; P=3878.71 Torr; 0.0833333 h;
参考文献
He, Hongjie; Lin, Qi; Liu, Xiaofeng; Yang, Yongtai; Zhou, Yaming; Jia, Yu; Gao, Xiang
Synthetic Communications, 2012 , vol. 42, # 17 p. 2512 - 2525
反应条件
1,10-phenanthroline; NiCl2(1,10-phenanthroline); methylmagnesium bromide; sodium t-butanolate in pyridine; diethyl ether
T=100°C; 21 h;
参考文献
Wolfe, John P.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1997 , vol. 119, # 26 p. 6054 - 6058
反应条件
sodium hydrogencarbonate in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=130°C;
参考文献
Juaristi, Eusebio; Madrigal, Domingo
Tetrahedron, 1989 , vol. 45, # 3 p. 629 - 636
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
potassium carbonate in water
T=100°C; 1 h; Microwave irradiation;
参考文献
Li, Hong Bo; Liang, Wu; Liu, Lang; Chen, Kai; Wu, Yi
Chinese Chemical Letters, 2011 , vol. 22, # 3 p. 276 - 279
反应条件
triethylsilane; [Ru(η4-COD)(η3-methylallyl)2]; trifluorormethanesulfonic acid; 1,5-bis-(diphenylphosphino)-pentane; triethylamine in 1,4-dioxane
24 h; Inert atmosphereReflux;
参考文献
Otsuka, Maiko; Endo, Kohei; Shibata, Takanori
Chemical Communications, 2010 , vol. 46, # 2 p. 336 - 338
反应条件
potassium hydroxide; pentacarbonyliron(0); carbon monoxide in ethanol; water
5 h; Ambient temperature;
参考文献
Shim, Sang Chul; Huh, Keun Tai; Park, Woo Hiun
Tetrahedron, 1986 , vol. 42, # 1 p. 259 - 264
反应条件
N-ethyl-N,N-diisopropylamine in toluene
Heating;
参考文献
Cheng; Zhan; Meth-Cohn
Synthesis, 2002 , # 1 p. 34 - 38
