5-氯-1(3h)-异苯并呋喃酮合成路线 (共 22 条)
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C
1.2: -78 - -15 °C
2.1: sodium tetrahydroborate / methanol / 5 h / Cooling with ice
3.1: hydrogenchloride / water / 6 h / Reflux
View Scheme
参考文献
Faigl, Ferenc; Thurner, Angelika; Molnar, Balazs; Simig, Gyula; Volk, Balazs
Organic Process Research and Development, 2010 , vol. 14, # 3 p. 617 - 622
反应条件
1: Br2 / CCl4 / Heating; irradiation
2: water / Heating
View Scheme
参考文献
Abaev, Vladimir T.; Dmitriev, Artem S.; Gutnov, Andrey V.; Podelyakin, Sergey A.; Butin, Alexander V.
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 5 p. 1195 - 1204