(2-氯苯基)(4-甲氧基苯基)甲酮合成路线 (共 12 条)
反应条件
copper ferrite in 1,2-dichloro-ethane T=35 - 38°C; Friedel-Crafts Acylation; 18 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
potassium phosphate; 3,3-dimethyl-butan-2-one; C14H10Cl2N2O2Ru; [(t-Bu)3PH]BF4 in water; toluene T=100°C; 24 h;
参考文献
Dey, Bikash Kali; Dutta, Jayita; Drew, Michael G.B.; Bhattacharya, Samaresh
Journal of Organometallic Chemistry, 2014 , vol. 750, p. 176 - 184
反应条件
sodium carbonate; palladium dichloride in water; acetone T=20°C; Suzuki type reaction; 1.5 h; Inert atmosphere;
参考文献
Xin, Bing-Wei
Synthetic Communications, 2008 , vol. 38, # 16 p. 2826 - 2837
反应条件
sodium lauryl sulfate; potassium carbonate; palladium dichloride in water T=60°C; 6 h;
参考文献
Xin, Bingwei; Zhang, Yuhong; Cheng, Kai
Synthesis, 2007 , # 13 p. 1970 - 1978
反应条件
potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=0°C; 9 h;
参考文献
Yoshida, Hiroto; Mimura, Yasuhiro; Ohshita, Joji; Kunai, Atsutaka
Chemical Communications, 2007 , # 23 p. 2405 - 2407
反应条件
tetrakis(triphenylphosphine) palladium(0); water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline in N,N-dimethyl-formamide T=60°C; 15 h; Inert atmosphere;
参考文献
Kwon, Young Bum; Choi, Bo Ram; Lee, Seung Hwan; Seo, Jin-Soo; Yoon, Cheol Min
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 9 p. 2672 - 2674
反应条件
3,3-dimethyl-butan-2-one; [Ru(CO)3Cl2]2; K3PO4*3H2O; [(t-Bu)3PH]BF4 in water; toluene T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Hong; Xu, Yuan; Shi, Erbo; Wei, Wei; Suo, Xiangqiang; Wan, Xiaobing
Chemical Communications, 2011 , vol. 47, # 27 p. 7880 - 7882
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 15 h;
参考文献
Chemistry - A European Journal, , vol. 18, # 24 p. 7486 - 7492
反应条件
1.1: magnesium / tetrahydrofuran / 1 h / Reflux 1.2: 0 °C / Inert atmosphere 2.1: pyridinium chlorochromate / dichloromethane / 15 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 24 p. 7486 - 7492
反应条件
1.1: magnesium / tetrahydrofuran / 1 h / Reflux 1.2: 0 °C / Inert atmosphere 2.1: pyridinium chlorochromate / dichloromethane / 15 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 24 p. 7486 - 7492