1-甲氧基-3-(三甲基硅氧基)-丁二烯合成路线 （共 70 条）
反应条件
in benzene T=65°C; 24 h;
参考文献
Jung, Michael E.; Grove, David D.
Journal of the Chemical Society, Chemical Communications, 1987 , p. 753 - 755
反应条件
Yield given. Multistep reaction;
参考文献
Hattori, Kouji; Yamamoto, Hisashi
Tetrahedron, 1993 , vol. 49, # 9 p. 1749 - 1760
反应条件
1: (S)-(-)-2,2-dimethyl-1,3-dioxolane-4-carboxaldehyde With (1R,2S) Jacobsen's chromium catalyst; BaO in ethyl acetate T=0 - 20°C; Inert atmosphere; 2: trans-1-methoxy-3-(trimethylsilyloxy)-1,3-butadiene in ethyl acetate T=0 - 4°C; hetero Diels-Alder reaction; DarknessInert atmosphere; 3: With trifluoroacetic acid in ethyl acetate T=0 - 20°C; Inert atmosphere; optical yield given as percent de;
参考文献
Smith III, Amos B.; Dong, Shuzhi
Organic Letters, 2009 , vol. 11, # 5 p. 1099 - 1102
反应条件
1: With BaO; (S,S)-(+)-Jacobsen salene complex in ethyl acetate T=0°C; hetero Diels-Alder reaction; 24 h; 2: With trifluoroacetic acid in dichloromethane; ethyl acetate T=0 - 20°C; 0.166667 h; Title compound not separated from byproducts;
参考文献
Paterson, Ian; Steven, Alan; Luckhurst, Chris A.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 20 p. 3026 - 3038
反应条件
in dichloromethane T=20°C;
参考文献
Mayr; Bug; Gotta; Hering; Irrgang; Janker; Kempf; Loos; Ofial; Remennikov; Schimmel
Journal of the American Chemical Society, 2001 , vol. 123, # 39 p. 9500 - 9512
反应条件
in chloroform-d1 T=55°C; 50 h; Title compound not separated from byproducts;
参考文献
Dowd, Paul; Weber, William
Journal of Organic Chemistry, 1982 , vol. 47, # 24 p. 4777 - 4779
反应条件
3 A molecular sieve; zinc(II) iodide in tetrahydrofuran T=20°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Abraham, Herve; Theus, Elisabeth; Stella, Lucien
Bulletin des Societes Chimiques Belges, 1994 , vol. 103, # 7-8 p. 361 - 366
反应条件
benzoic acid T=20°C;
参考文献
Acocella, Maria Rosaria; Massa, Antonio; Palombi, Laura; Villano, Rosaria; Scettri, Arrigo
Tetrahedron Letters, 2005 , vol. 46, # 36 p. 6141 - 6144
反应条件
Ce(III)-(R)-BNP in dichloromethane T=20°C; asymmetric hetero-Diels-Alder reaction; 15 h;
参考文献
Hayano, Tetsuji; Sakaguchi, Toshiaki; Furuno, Hiroshi; Ohba, Masaaki; Okawa, Hisashi; Inanaga, Junji
Chemistry Letters, 2003 , vol. 32, # 7 p. 608 - 609
反应条件
(scandium(III))2(biphenyl-4,4'-disulfonate)3 T=20°C; Diels-Alder reaction;
参考文献
Ishida, Shuichi; Hayano, Tetsuji; Furuno, Hiroshi; Inanaga, Junji
Heterocycles, 2005 , vol. 66, # 1 p. 645 - 649
