1-甲氧基-3-(三甲基硅氧基)-丁二烯合成路线 （共 70 条）
参考文献
Gupta, Y. N.; Mani, S. R.; Houk, K. N.
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 495 - 498
反应条件
1: in benzene Diels-Alder reaction; 23 h; Heating; 2: With acetic acid T=20°C; 24 h; 3: With potassium tert-butylate in tetrahydrofuran 2 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 15 p. 1794 - 1799
参考文献
Houge-Frydrych, Catherine S.V.; Motherwell, William B.; O'Shea, Dennis M.
Heterocycles, 1989 , vol. 28, # 2 p. 603 - 606
反应条件
in dichloromethane T=80°C; P=9000720 Torr; 72 h;
参考文献
Heterocycles, , vol. 56, # 1-2 p. 209 - 220
反应条件
1: With titanium(IV) isopropylate; (R)-(+)-5,5',6,6',7,7',8,8'-octahydro-bi-2-naphthol in toluene T=0°C; hetero-Diels-Alder reaction; 24 h; 2: With trifluoroacetic acid in toluene T=0°C; 0.25 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 7 p. 2175 - 2182
反应条件
1: cyclopent-2-enone With zinc(II) chloride in tetrahydrofuran Diels-Alder reaction; 0.25 h; 2: trans-1-methoxy-3-(trimethylsilyloxy)-1,3-butadiene in dichloromethane T=22°C; Diels-Alder reaction; 168 h; 3: With hydrogenchloride in water T=20°C;
参考文献
Krebs, Michael; Laschat, Sabine
Arkivoc, 2012 , vol. 2012, # 3 p. 5 - 19
反应条件
in benzene T=140°C; Diels-Alder cycloaddition reaction; 72 h; Cooling with liquid nitrogensealed;
参考文献
Della Rosa, Claudia D.; Sanchez, Juan P.; Kneeteman, Maria N.; Mancini, Pedro M.E.
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2316 - 2319
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Corey, E. J.; Estreicher, Herbert
Tetrahedron Letters, 1981 , vol. 22, p. 603 - 606
反应条件
1: With scandium tris(trifluoromethanesulfonate) in acetonitrile T=0°C; Diels-Alder reaction; 0.05 h; 2: With water in acetonitrile Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 344, # 5 p. 548 - 555
反应条件
in dichloromethane T=40°C; Cycloaddition; P=9000720 Torr; 50 h;
参考文献
Tetrahedron Letters, , vol. 41, # 42 p. 8079 - 8082
