1-甲氧基-3-(三甲基硅氧基)-丁二烯合成路线 （共 70 条）
反应条件
N-methylimidazolium hexafluorophosphate T=60°C; 48 h; Sealed tubeInert atmosphere; Reagent/catalystTime;
参考文献
Mancini, Pedro M. E.; Rosa, Claudia D. Della; Ormachea, Carla M.; Kneeteman, Maria N.; Domingo, Luis R.
RSC Advances, 2013 , vol. 3, # 33 p. 13825 - 13834
反应条件
in benzene T=120°C; Diels-Alder reaction; 72 h;
参考文献
Rosa, Claudia Della; Kneeteman, Maria N.; Mancini, Pedro M.E.
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8711 - 8714
参考文献
Corey, E. J.; Estreicher, Herbert
Tetrahedron Letters, 1981 , vol. 22, p. 603 - 606
反应条件
1: With bismuth(III) chloride in dichloromethane T=20°C; 12 h; 2: With hydrogen; palladium on activated charcoal
参考文献
Tetrahedron Letters, , vol. 43, # 9 p. 1645 - 1648
反应条件
in benzene T=120°C; Diels-Alder reaction; 72 h;
参考文献
Rosa, Claudia Della; Kneeteman, Maria N.; Mancini, Pedro M.E.
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8711 - 8714
反应条件
ytterbium(III) triflate in acetonitrile Diels-Alder reaction; 1 h;
参考文献
Creswell, Mark W.; Bolton, Gary L.; Hodges, John C.; Meppen, Malte
Tetrahedron, 1998 , vol. 54, # 16 p. 3983 - 3998
反应条件
zinc(II) chloride in dichloromethane T=30°C; 0.0333333 h; Microwave irradiationSealed vessel;
参考文献
Burland, Peter A.; Coisson, David; Osborn, Helen M. I.
Journal of Organic Chemistry, 2010 , vol. 75, # 21 p. 7210 - 7218
反应条件
butylmethylimidazolium triflate T=30°C; aza-Diels-Alder reaction; 1 h;
参考文献
Pegot, Bruce; Vo-Thanh, Giang
Synlett, 2005 , # 9 art. no. D05305ST, p. 1409 - 1412
反应条件
1: benzaldehyde With Rinkamide(aminomethyl)polystyrene-resin; trimethyl orthoformate T=20°C; 18 h; 2: trans-1-methoxy-3-(trimethylsilyloxy)-1,3-butadiene With ytterbium(III) triflate in tetrahydrofuran T=0 - 20°C; hetero-Diels-Alder reaction; 20 h; 3: With acetic acid in dichloromethane T=20°C; 3 h;
参考文献
Tetrahedron, , vol. 61, # 1 p. 205 - 211
反应条件
1: benzonitrile With lithium triethylborohydride in tetrahydrofuran T=20°C; 1.5 h; 2: trans-1-methoxy-3-(trimethylsilyloxy)-1,3-butadiene in tetrahydrofuran T=20°C; 5 h;
参考文献
Synthesis, , # 6 p. 828 - 830
