1-甲氧基-3-(三甲基硅氧基)-丁二烯合成路线 （共 70 条）
反应条件
in benzene
25 °C, 3-5 d, 800 psi CO;
参考文献
Wulff, William D.; Yang, Dominic C.; Murray, Christopher K.
Pure and Applied Chemistry, 1988 , vol. 60, p. 137 - 144
反应条件
in benzene
3 h; Heating;
参考文献
Ameer; Green, Ivan R.; Krohn; Sitoza
Synthetic Communications, 2007 , vol. 37, # 18 p. 3041 - 3057
反应条件
toluene-4-sulfonic acid
1.) C6H6, reflux, 48 h, 2.) C6H6, reflux, 16 h; Yield given. Multistep reaction;
参考文献
Jung; Rayle
Synthetic Communications, 1994 , vol. 24, # 2 p. 197 - 203
反应条件
1: in benzene
T=50°C; Diels-Alder cycloaddition; 72 h;
2: With acetic acid; zinc
T=20°C; Reduction; aromatization;
3: With aluminium trichloride; sodium chloride
T=140°C; demethylation;
参考文献
Cameron, Donald W.
Australian Journal of Chemistry, 1999 , vol. 52, # 12 p. 1165 - 1171
反应条件
triethylamine
1) benzene, reflux, 2) CH2Cl2, 5 min.; Yield given. Multistep reaction;
参考文献
Beagley, Brian; Curtis, Anthony D. M.; Pritchard, Robin G.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 15 p. 1981 - 1991
反应条件
triethylamine in dichloromethane
T=25°C; Yield given;
参考文献
Spino, Claude; Crawford, Jason; Cui, Yunping; Gugelchuk, Melinda
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 6 p. 1499 - 1506
反应条件
in toluene
4 h; Heatingvarious reagent ratios; Product distribution;
参考文献
Spino, Claude; Crawford, Jason; Cui, Yunping; Gugelchuk, Melinda
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 6 p. 1499 - 1506
反应条件
1: With (R)-H4-BINOL and (R)-H8 BINOL Ti(IV)
T=20°C; hetero-Diels-Alder reaction; 48 h;
2: With trifluoroacetic acid
T=20°C; Further stages.;
参考文献
Yuan, Yu; Long, Jiang; Sun, Jie; Ding, Kuiling
Chemistry - A European Journal, 2002 , vol. 8, # 21 p. 5033 - 5042
参考文献
Danishefsky,S.; Kitahara,T.
Journal of the American Chemical Society, 1974 , vol. 96, p. 7807 - 7808
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Danishefsky,S. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 6996 - 7000
反应条件
(i), (ii) H+; Multistep reaction;
参考文献
Semmelhack; Sarpong, Richmond; Bergman, Jeffrey; Ho, Douglas M.
Tetrahedron Letters, 2002 , vol. 43, # 4 p. 541 - 544
