3,5-二甲基苯基异氰酸酯合成路线 （共 7 条）
反应条件
sodium hydrogencarbonate in dichloromethane; water; toluene T=0 - 20°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 17, # 23 p. 8102 - 8112
反应条件
1: trimethylsilylazide; tert.-butylnitrite / acetonitrile / 1 h / 0 - 20 °C / |Inert atmosphere; |Cooling with ice 2: diethyl ether / 3 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organometallics, , vol. 32, # 8 p. 2300 - 2308
反应条件
carbon in ethyl acetate Condensation; Heating;
参考文献
Pharmazie, , vol. 55, # 2 p. 83 - 86
反应条件
in dichloromethane T=15°C; Reflux;
参考文献
Asian Journal of Chemistry, , vol. 23, # 4 p. 1802 - 1806
反应条件
in diethyl ether T=20°C; 3 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 8 p. 2300 - 2308
参考文献
Chemische Berichte, , vol. 25, p. 1089
反应条件
in hexane
Ambient temperature;
参考文献
DeVries, Vern G.; Bloom, Jonathan D.; Dutia, Minu D.; Katocs, Andrew S.; Largis, Elwood E.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 10 p. 2318 - 2325
